The LAD (large area detector) instrument, onboard the Sino-European mission eXTP (enhanced x-ray timing and polarimetry), will perform single-photon, high-resolution timing and energy measurements, in the energy range 2 to 30 keV, with a large collecting area. Its silicon drift detectors need shielding from NIR/Vis/UV light by astrophysical sources and the bright Earth, to avoid performance degradation. Filters made of an Al coated thin polyimide (PI) membrane will guarantee the needed out-of-band rejection while offering high x-ray transparency. They will be placed between the detectors and the capillary plate plate collimators, open to the external environment. The mission is now in phase B2 and a baseline design for the filters was produced. We describe the filter design and modeling activity, and report the characterization performed so far on x-ray transmission, pinhole and defects, thermo-vacuum cycling endurance, and bright Earth optical load shielding properties.
In this paper, we present the first results from an investigation performed on nanometric thin pellicles based on carbon nanotubes (CNT) of potential interest for manufacturing large area optical blocking filters to protect soft x-ray detectors in astrophysics space missions. In order to evaluate the effective capability of such materials to block UV/VIS/IR radiation, while being highly transparent in the soft x-rays and strong enough to withstand the severe launch stresses, we have performed a suite of characterization measurements. These include: UV/VIS/IR and x-ray absorption spectroscopy, x-ray photoelectron spectroscopy and scanning electron microscopy on bare and Al coated small self-standing pellicles; static mechanical tests on small freestanding samples.
Advanced Telescope for High-Energy Astrophysics is a large-class astrophysics space mission selected by the European Space Agency to study the theme “Hot and Energetic Universe.” The mission essentially consists of a large effective area x-ray telescope and two detectors: the X-ray Integral Field Unit (X-IFU) and the Wide Field Imager (WFI). Both instruments require filters to shield from out-of-band radiation while providing high transparency to x-rays. The mission is presently in phase B; thus, to consolidate the preliminary design, investigated filter materials need to be properly characterized by experimental test campaigns. We report results from high-resolution x-ray transmission measurements performed using different synchrotron radiation beamlines to assess the filter calibration accuracy and mitigate the risk related to selecting a unique calibration facility. The main goals of these test campaigns are (i) to verify the compliance of the investigated filter design to the scientific requirements, (ii) to develop an accurate x-ray transmission model, and (iii) to start identifying suitable measurement facilities and achievable accuracy for the flight filters calibration program. In particular, the x-ray transmission model of the X-IFU and WFI filters has been refined within the edges of Al, C, N, and O by deriving the optical constants from two reference samples measured by synchrotron light. The achievable filter calibration accuracy has been estimated by evaluating the agreement between the best-fit according to the developed transmission model and the experimental data.
Single sensors or small arrays of manually assembled neutron transmutation doped germanium (NTD-Ge) based microcalorimeters have been widely used as high energy-resolution detectors from infrared to hard X-rays. Several planar technological processes were developed in the last years aimed at the fabrication of NTD-Ge arrays, specifically designed to produce soft X-ray detectors. One of these processes consists in the fabrication of the absorbers. In order to absorb efficiently hard X-ray photons, the absorber has to be properly designed and a suitable material has to be employed. Bismuth offers interesting properties in terms of absorbing capability, of low heat capacity (needed to obtain high energy resolution) and deposition technical feasibility, moreover, it has already been used as absorber for other types of microcalorimeters. Here we present the electroplating process we adopted to grow bismuth absorbers for fabricating planar microcalorimeter arrays for hard X-rays detection. The process was specifically tuned to grow uniform Bi films with thickness up to ~ 70 μm. This work is part of a feasibility study for a stratospheric balloon borne experiment that would observe hard X-rays (20-100 keV) from solar corona.
The Wide Field Imager (WFI) is one of the two instruments of the ATHENA astrophysics space mission approved by ESA as the second large mission in the Cosmic Vision 2015-2025 Science Programme. The WFI, based on a large array of depleted field effect transistors (DEPFET), will provide imaging in the 0.2-15 keV band over a 40’x40’ field of view, simultaneously with spectrally and time resolved photon counting. The WFI detector is also sensitive to UV/Vis photons, with an electron-hole pair production efficiency in the UV/VIS larger than that for X-ray photons. Optically generated photo-electrons may degrade the spectral resolution as well as change the energy scale by introducing a signal offset. For this reason, the use of X-ray transparent optical blocking filters (OBFs) are needed to allow the observation of X-ray sources that present a UV/Vis bright counterpart. The OBFs design is challenging since one of the two required filters is quite large (~ 160 mm × 160 mm), very thin (< 200 nm), and shall survive the mechanical load during the launch. In this paper, we review the main results of modeling and characterization tests of OBF partially representative samples, performed during the phase A study, to identify the suitable materials, optimize the design, prove that the filters can be launched in atmospheric pressure, and thus demonstrate that the chosen technology can reach the proper technical readiness before mission adoption.
The X-ray Integral Field Unit (X-IFU) is one of the two instruments of the Athena astrophysics space mission approved by ESA in the Cosmic Vision 2015-2025 Science Programme. The X-IFU consists of a large array of transition edge sensor micro-calorimeters that will operate at ~100 mK inside a sophisticated cryostat. A set of thin filters, highly transparent to X-rays, will be mounted on the opening windows of the cryostat thermal shields in order to attenuate the IR radiative load, to attenuate radio frequency electromagnetic interferences, and to protect the detector from contamination. Thermal filters are critical items in the proper operation of the X-IFU detector in space. They need to be strong enough to survive the launch stresses but very thin to be highly transparent to X-rays. They essentially define the detector quantum efficiency at low energies and are fundamental to make the photon shot noise a negligible contribution to the energy resolution budget. In this paper, we review the main results of modeling and characterization tests of the thermal filters performed during the phase A study to identify the suitable materials, optimize the design, and demonstrate that the chosen technology can reach the proper readiness before mission adoption.
The X-ray Integral Field Unit (X-IFU) is one of the two detectors of the ATHENA astrophysics space mission approved by ESA in the Cosmic Vision 2015-2025 Science Programme. The X-IFU consists of a large array of transition edge sensors (TES) micro-calorimeters covering a field of view of ~5’ diameter, sensitive in the energy range 0.2-12 keV, and providing a spectral resolution of 2.5 eV at 7 keV. Both the TES and superconducting quantum interference devices (SQUID) based read-out electronics are very sensitive to electromagnetic interferences (EMI), and a proper shielding of the focal plane assembly (FPA) is required to prevent a deterioration of the energy resolution. A set of thin filters, highly transparent to X-rays, will be mounted on the FPA and on the cryostat thermal shields in order to attenuate the infrared radiative load, and to protect the detector from contamination. Some of these filters are also aimed at providing proper radio frequency (RF) shielding in the frequency range of the satellite telemetry downlink antenna. In addition, filters should also be effective in shielding any RF interference generated by other on-board electronics. In this paper, we present results from RF measurements performed on thin plastic foils coated with an aluminum layer, with and without metal meshes, and identify the filter characteristics matching the RF shielding requirements.
ATHENA is a Large high energy astrophysics space mission selected by ESA in the Cosmic Vision 2015-2025 Science Program. It will be equipped with two interchangeable focal plane detectors: the X-Ray Integral Field Unit (X-IFU) and the Wide Field Imager (WFI). Both detectors require x-ray transparent filters to fully exploit their sensitivity. In order to maximize the X-ray transparency, filters must be very thin, from a few tens to few hundreds of nm, on the other hand, they must be strong enough to survive the severe launch stresses. In particular, the WFI OBF, being launched in atmospheric pressure, shall also survive acoustic loads. In this paper, we present a review of the structural modeling performed to assist the ATHENA filters design, the preliminary results from vibration and acoustic tests, and we discuss future activities necessary to consolidate the filters design, before the preliminary requirement review of the ATHENA instruments, scheduled before the end of 2018.
The X-IFU instrument of the ATHENA mission requires a set of thermal filters to reduce the photon shot noise onto its cryogenic detector and to protect it from molecular contamination. A set of five filters, operating at different nominal temperatures corresponding to the cryostat shield temperatures, is currently baselined. The knowledge of the actual filter temperature profiles is crucial to have a good estimation of the radiative load on the detector. Furthermore, a few filters may need to be warmed-up to remove contaminants and it is necessary to ensure that a threshold temperature is reached throughout the filters surface. For these reasons, it is fundamental to develop a thermal modeling of the full set of filters in a representative configuration. The baseline filter is a polyimide membrane 45 nm thick coated with 30 nm of highpurity aluminum, mechanically supported by a metallic honeycomb mesh. In this paper, we describe the implemented thermal modeling and report the results obtained in different studies: (i) a trade-off analysis on how to reach a minimum target temperature throughout the outer filter, (ii) a thermal analysis when varying the emissivity of the filter surfaces, and (iii) the effect of removing one of the filters.
A technique to obtain lightweight and high-resolution focusing mirror segments for large aperture X-ray telescopes is the
hot slumping of thin glass foils. In this approach, already successfully experimented to manufacture the optics of the
NuSTAR X-ray telescope, thin glasses are formed at high temperature onto a precisely figured mould. The formed glass
foils are subsequently stacked onto a stiff backplane with a common axis and focus to form an XOU (X-ray Optical Unit),
to be later integrated in the telescope optic structure. In this process, the low thickness of the glass foils guarantees a low
specific mass and a very low obstruction of the effective area. However, thin glasses are subject to deformations that may
arise at any stage of the production process, thereby degrading the angular resolution. To solve this problem, several groups
are working on the possibility to correct the mirror profile post-manufacturing, using piezoelectric elements exerting a
tangential strain on the non-optical side of the glass mirrors. In this paper we show the results of the approach we have
adopted, based on the application of piezoceramic patches on the backside of thin glass foils, previously formed by hot
slumping. The voltage signals are supplied to the piezoelectric elements by a system of electrodes deposited on the same
side of the mirror via a photolithographic process. Finally, the matrix of voltages to be used to correct the mirror shape can
be determined in X-rays illumination by detection of the intra-focal image and consequent reconstruction of the
longitudinal profile. We describe the production of some active mirrors with different arrangements of piezoelectric
elements and the X-ray tests performed at the XACT X-ray facility to determine the optimal actuator geometry.
Use of thin glass modular optics is a technology currently under study to build light, low cost, large area X-ray telescopes for high energy astrophysics space missions. The angular resolution of such telescopes is limited by local deviations from the ideal shape of the mirrors. One possible strategy to improve it consists in actively correcting the mirror profile by gluing thin ceramic piezo-electric actuators on the back of the glasses. A large number of actuators, however, requires several electrical connections to drive them with the different needed voltages. We have developed a process for depositing conductive paths directly on the back of non-planar thin foil mirrors by means of a photolithographic process, combined with metal thin film evaporation and selective removal. We have also designed and built a modular multichannel electronic driver with each module capable of driving simultaneously up to 16 actuators with a very low power consumption. Here we present our electrical interconnections technology and the solutions adopted in the implementation of the electronics.
The X-Ray Integral Field Unit (X-IFU) detector on-board ATHENA is an array of TES micro-calorimeters that will operate at ~50 mK. In the current investigated design, five thermal filters (TF) will be mounted on the cryostat shields to attenuate IR radiative load and avoid energy resolution degradation due to photon shot noise. Each filter consists of a thin polyimide film (~50 nm thick) coated with aluminum (~30 nm thick).
Since the TF operate at different temperatures in the range 0.05-300 K, it is relevant to study how temperature affects their mechanical/optical performances (e.g. near edge absorption fine structures of the atomic elements in the filter material). Such results are crucial for the proper design of the filters as well as to establish the calibration program operating temperatures.
We report the preliminary results of visual inspections performed on test filters of polyimide/Al at different pressure and temperature conditions, IR transmission measurements (1-15 μm) performed in the temperature range 10- 300 K, and X-ray Absorption Spectroscopy measurements (175-1650 eV) performed in the temperature range 130-300 K.
The ATHENA mission provides the demanded capabilities to address the ESA science theme "Hot and Energetic Universe". Two complementary instruments are foreseen: the X-IFU (X-ray Integral Field Unit) and WFI (Wide Field Imager). Both the instruments require filters to avoid that the IR radiation heats the X-IFU cryogenic detector and to protect the WFI detector from UV photons. Previous experience on XMM filters recommends to employ bilayer membrane consisting of aluminum deposited on polyimide. In this work, we use the X-ray Photoelectron Spectroscopy (XPS) to quantify the native aluminum oxide thickness that affects the spectral properties of the filter. The estimation of the oxide thickness of the prototype filter for ATHENA is a considerable information for the conceptual design of the filters.
Optics for future X-ray telescopes will be characterized by very large aperture and focal length, and will be made of lightweight materials like glass or silicon in order to keep the total mass within acceptable limits. Optical modules based on thin slumped glass foils are being developed at various institutes, aiming at improving the angular resolution to a few arcsec HEW. Thin mirrors are prone to deform, so they require a careful integration to avoid deformations and even correct forming errors. On the other hand, this offers the opportunity to actively correct the residual deformation: a viable possibility to improve the mirror figure is the application of piezoelectric actuators onto the non-optical side of the mirrors, and several groups are already at work on this approach. The concept we are developing consists of actively integrating thin glass foils with piezoelectric patches, fed by voltages driven by the feedback provided by X-rays. The actuators are commercial components, while the tension signals are carried by a printed circuit obtained by photolithography, and the driving electronic is a multi-channel low power consumption voltage supply developed inhouse. Finally, the shape detection and the consequent voltage signal to be provided to the piezoelectric array are determined in X-rays, in intra-focal setup at the XACT facility at INAF/OAPA. In this work, we describe the manufacturing steps to obtain a first active mirror prototype and the very first test performed in X-rays.
ATHENA is the L2 mission selected by ESA to pursue the science theme “Hot and Energetic Universe” (launch scheduled in 2028). One of the key instruments of ATHENA is the Wide Field Imager (WFI) which will provide imaging in the 0.1-15 keV band over a 40’x40’ large field of view, together with spectrally and time-resolved photon counting. The WFI camera, based on arrays of DEPFET active pixel sensors, is also sensitive to UV/Vis photons. Optically generated electron-hole pairs may degrade the spectral resolution as well as change the energy scale by introducing a signal offset. For this reason, the use of an X-ray transparent optical blocking filter is needed to allow the observation of all type of X-ray sources that present a UV/Visible bright counterpart. In this paper, we describe the main activities that we are carrying on for the conceptual design of the optical blocking filter, that will be mounted on the filter wheel, in order to satisfy the scientific requirements on optical load from bright UV/Vis astrophysical source, to maximize the X-ray transmission, and to withstand the severe acoustic and vibration loads foreseen during launch.
Optics for future X-ray telescopes will be characterized by very large aperture and focal length, and will be made of
lightweight materials like glass or plastic in order to keep the total mass within acceptable limits. Optics based on thin
slumped glass foils are currently in use in the NuSTAR telescope and are being developed at various institutes like
INAF/OAB, aiming at improving the angular resolution to a few arcsec HEW. Another possibility would be the use of
thin plastic foils, being developed at SAO and the Palermo University. Even if relevant progresses in the achieved
angular resolution were recently made, a viable possibility to further improve the mirror figure would be the application
of piezoelectric actuators onto the non-optical side of the mirrors. In fact, thin mirrors are prone to deform, so they
require a careful integration to avoid deformations and even correct forming errors. This however offers the possibility to
actively correct the residual deformation. Even if other groups are already at work on this idea, we are pursuing the
concept of active integration of thin glass or plastic foils with piezoelectric patches, fed by voltages driven by the
feedback provided by X-rays, in intra-focal setup at the XACT facility at INAF/OAPA. In this work, we show the
preliminary simulations and the first steps taken in this project.
After more than ten years of operation of the EPIC camera on board the X-ray observatory XMM-Newton, we have
reviewed the status of its Thin and Medium filters by performing both laboratory measurements on back-up filters, and
analysis of data collected in-flight.
We have selected a set of Thin and Medium back-up filters among those still available in the EPIC consortium, and have
started a program to investigate their status by different laboratory measurements including: UV/VIS transmission, X-ray
transmission, RAMAN IR spectroscopy, X-Ray Photoelectron Spectroscopy, and Atomic Force Microscopy. We report
the results of the measurements conducted up to now, and point out some lessons learned for the development and
calibration programs of filters for X-ray detectors in future Astronomy missions.
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