Thin films on the nanoscale represent a solution to the balance between a nanomaterial of beneficial architectural properties and one of functional chemical properties. Due to the size range involved, XPS and related techniques represent an obvious analytical process by which to investigate these films. Here, typical and atypical use of XPS, along with REELS, ISS and several additional techniques is discussed in order to fully explore synthetical procedures and new materials in the development of advanced functional materials for fields such as catalysis and medical devices.
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