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Small scale magnets have very high technological importance today. We synthesized thin film magnets containing iron and nickel oxides using sol-gel and spin coating methods. Structural properties of iron particles were investigated using Mossbauer spectroscopy, X-ray absorption spectroscopy including Extended X-ray Absorption Spectroscopy. The variation in oxidation state and other structural parameters were deduced. It appears the oxidation state of iron particles prepared by sol-gel method is very stable up to annealing temperatures of 600° C. The iron particles prepared by spin coating method exist in two different chemical environments with slightly different oxidation states.
Sunil Dehipawala,Pubudu Samarasekara,Khushpreet Kaur, andHarsha Rajapakse
"Comparison of structural properties of iron nano-particles prepared by sol-gel method and spin coating technique", Proc. SPIE 10731, Nanostructured Thin Films XI, 107310T (7 September 2018); https://doi.org/10.1117/12.2320410
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Sunil Dehipawala, Pubudu Samarasekara, Khushpreet Kaur, Harsha Rajapakse, "Comparison of structural properties of iron nano-particles prepared by sol-gel method and spin coating technique," Proc. SPIE 10731, Nanostructured Thin Films XI, 107310T (7 September 2018); https://doi.org/10.1117/12.2320410